Junyang Li, Roberta Campardelli, Giuseppe Firpo, 等. Oil-in-water nanoemulsions loaded with lycopene extracts encapsulated by spray drying: Formulation, characterization and optimization[J]. 中国化学工程学报(英文版), 2024,70(6):73-81.
Junyang Li, Roberta Campardelli, Giuseppe Firpo, Jingtao Zhang, Patrizia Perego. Oil-in-water nanoemulsions loaded with lycopene extracts encapsulated by spray drying: Formulation, characterization and optimization[J]. Chinese Journal of Chemical Engineering, 2024, 70(6): 73-81.
Junyang Li, Roberta Campardelli, Giuseppe Firpo, 等. Oil-in-water nanoemulsions loaded with lycopene extracts encapsulated by spray drying: Formulation, characterization and optimization[J]. 中国化学工程学报(英文版), 2024,70(6):73-81.DOI: 10.1016/j.cjche.2024.03.002.
Junyang Li, Roberta Campardelli, Giuseppe Firpo, Jingtao Zhang, Patrizia Perego. Oil-in-water nanoemulsions loaded with lycopene extracts encapsulated by spray drying: Formulation, characterization and optimization[J]. Chinese Journal of Chemical Engineering, 2024, 70(6): 73-81.DOI: 10.1016/j.cjche.2024.03.002.
Oil-in-water nanoemulsions loaded with lycopene extracts encapsulated by spray drying: Formulation, characterization and optimization
Lycopene is very susceptible to degradation once released from the protective chromoplast environment. In this study
oil-in-water (O/W) nanoemulsions coupled with spray drying technology were applied for the encapsulation and stabilization of lycopene extracted from tomato waste. Tomato extract was obtained by ultrasound-assisted extraction. Nanoemulsions were prepared by a high-speed rotor stator using isopropyl myristate as the oil phase and Pluronic F-127 as the emulsifier for the aqueous external phase. The effect of emulsification process parameters was investigated. Spray drying of the produced emulsions was attempted to obtain a stabilized dry powder after the addition of a coating agent. The effect of different coating agents (maltodextrin
inulin
gum arabic
pectin
whey and polyvinylpyrrolidone)
drying temperature (120-170 ℃)
and feed flow rate (3-9 ml·min
-1
) on the obtained particles was evaluated. Results revealed that the emulsion formulation of 20/80 (O/W) with 1.5% (mass fraction) of Pluronic F-127 as stabilizer in the aqueous phase resulted in a stable nanoemulsion with droplet sizes in the range of 259-276 nm with a unimodal and sharp size distribution. The extract in the nanoemulsion was well protected at room temperature with a degradation rate of lycopene of about 50% during a month of storage time. The most stable emulsions were then processed by spray drying to obtain a dry powder. Spray drying was particularly successful when using maltodextrin as a coating agent
obtaining dried spherical particles with mean diameters of μm with a smooth surface. The possibility of dissolving the spray dried powder in order to repristinate. The or
iginal emulsion was also successfully verified.
Abstract
Lycopene is very susceptible to degradation once released from the protective chromoplast environment. In this study
oil-in-water (O/W) nanoemulsions coupled with spray drying technology were applied for the encapsulation and stabilization of lycopene extracted from tomato waste. Tomato extract was obtained by ultrasound-assisted extraction. Nanoemulsions were prepared by a high-speed rotor stator using isopropyl myristate as the oil phase and Pluronic F-127 as the emulsifier for the aqueous external phase. The effect of emulsification process parameters was investigated. Spray drying of the produced emulsions was attempted to obtain a stabilized dry powder after the addition of a coating agent. The effect of different coating agents (maltodextrin
inulin
gum arabic
pectin
whey and polyvinylpyrrolidone)
drying temperature (120-170 ℃)
and feed flow rate (3-9 ml·min
-1
) on the obtained particles was evaluated. Results revealed that the emulsion formulation of 20/80 (O/W) with 1.5% (mass fraction) of Pluronic F-127 as stabilizer in the aqueous phase resulted in a stable nanoemulsion with droplet sizes in the range of 259-276 nm with a unimodal and sharp size distribution. The extract in the nanoemulsion was well protected at room temperature with a degradation rate of lycopene of about 50% during a month of storage time. The most stable emulsions were then processed by spray drying to obtain a dry powder. Spray drying was particularly su
ccessful when using maltodextrin as a coating agent
obtaining dried spherical particles with mean diameters of μm with a smooth surface. The possibility of dissolving the spray dried powder in order to repristinate. The original emulsion was also successfully verified.
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