Preparation of new and novel wave like poly(2-anisidine) zirconium tungstate nanocomposite: Thermal, electrical and ion-selective studies

Anish Khan; Aftab Aslam Parwaz Khan; Mahmoud A. Hussein; Bernaurdshaw Neppolian; Abdullah M. Asiri

doi:10.1016/j.cjche.2018.03.028

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Preparation of new and novel wave like poly(2-anisidine) zirconium tungstate nanocomposite: Thermal, electrical and ion-selective studies

Energy, Resources and Environmental Technology | Updated：2026-01-06

- Preparation of new and novel wave like poly(2-anisidine) zirconium tungstate nanocomposite: Thermal, electrical and ion-selective studies
- Preparation of new and novel wave like poly(2-anisidine) zirconium tungstate nanocomposite: Thermal, electrical and ion-selective studies
- 中国化学工程学报（英文版） 2019年27卷第2期页码：459-466
- Affiliations：
  
  1. 2 Center of Excellence for Advanced Materials Research, King Abdulaziz University, P.O. Box 80203, Jeddah 21589, Saudi Arabia
  2. 3 Polymer Chemistry Laboratory, Chemistry Department, Faculty of Science, Assiut University, Assiut,Egypt,71516
  3. 4 SRM Research Institute, SRM University, Kattankulathur, Chennai 603203, Tamil Nadu,India
- Author bio：
- Funds：
- DOI：10.1016/j.cjche.2018.03.028
  中图分类号：
- 纸质出版：2019
- Accepted：
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Anish Khan, Aftab Aslam Parwaz Khan, Mahmoud A. Hussein, 等. Preparation of new and novel wave like poly(2-anisidine) zirconium tungstate nanocomposite: Thermal, electrical and ion-selective studies[J]. 中国化学工程学报（英文版）, 2019,27(2):459-466.

Anish Khan, Aftab Aslam Parwaz Khan, Mahmoud A. Hussein, Bernaurdshaw Neppolian, Abdullah M. Asiri. Preparation of new and novel wave like poly(2-anisidine) zirconium tungstate nanocomposite: Thermal, electrical and ion-selective studies[J]. Chin.J.Chem.Eng., 2019, 27(2): 459-466.
Anish Khan, Aftab Aslam Parwaz Khan, Mahmoud A. Hussein, 等. Preparation of new and novel wave like poly(2-anisidine) zirconium tungstate nanocomposite: Thermal, electrical and ion-selective studies[J]. 中国化学工程学报（英文版）, 2019,27(2):459-466. DOI： 10.1016/j.cjche.2018.03.028.

Anish Khan, Aftab Aslam Parwaz Khan, Mahmoud A. Hussein, Bernaurdshaw Neppolian, Abdullah M. Asiri. Preparation of new and novel wave like poly(2-anisidine) zirconium tungstate nanocomposite: Thermal, electrical and ion-selective studies[J]. Chin.J.Chem.Eng., 2019, 27(2): 459-466. DOI： 10.1016/j.cjche.2018.03.028.

摘要

Abstract

It is necessary to synthesize new material for the advancements of the technology. In this study

new and novel poly (2-anisidine)@zirconium tungstate (P2A/ZrW

) was synthesized by simple so-gel method. Physicochemical characterization of P2A/ZrW

was done by thermogravimetric analysis (TGA)

scanning electron microscopy (SEM)

X-ray powder diffraction (XRD)

Fourier transform infrared spectroscopy (FTIR)

ion exchange and simultaneous four probe dc conductivity studies. The conductivity study revealed its highly semiconducting nature

in the range of 10

-1

-10

-2

S·cm

-1

. Ion-exchange capabilities of the composite make it applicable for cation-exchange studies. The result of distribution studies (K

) revealed its selectivity towards Cd

compared to other metal ions. This property of the composite was utilized for designing Cd

selective membrane electrode. Several important physical parameters of the ion-selective electrode were determined

such as Nernstian slope (32.32 mV·decade

-1

)

working pH range was 2

.0-4.0 and response time was found~17 s. The analytical utility of this wave like composite membrane electrode was as

indicator electrode in various potentiometric titrations.

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