Preparation and characterization of monodisperse zirconia spherical nanometer powder via lamellar liquid crystal template method

Weiyan He; Jinrong Liu; Zhenzhu Cao; Caihong Li; Yanfang Gao

doi:10.1016/j.cjche.2015.08.032

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Preparation and characterization of monodisperse zirconia spherical nanometer powder via lamellar liquid crystal template method

材料与产品工程 | Updated：2026-01-06

- Preparation and characterization of monodisperse zirconia spherical nanometer powder via lamellar liquid crystal template method
- Preparation and characterization of monodisperse zirconia spherical nanometer powder via lamellar liquid crystal template method
- 中国化学工程学报（英文版） 2015年23卷第10期页码：1721-1727
- Affiliations：
  
  School of Chemical Engineering, Inner Mongolia University of Technology,Hohhot,China,010051
- Author bio：
- Funds：
- DOI：10.1016/j.cjche.2015.08.032
  中图分类号：
- 纸质出版：2015
- Accepted：
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Weiyan He, Jinrong Liu, Zhenzhu Cao, 等. Preparation and characterization of monodisperse zirconia spherical nanometer powder via lamellar liquid crystal template method[J]. 中国化学工程学报（英文版）, 2015,23(10):1721-1727.

Weiyan He, Jinrong Liu, Zhenzhu Cao, Caihong Li, Yanfang Gao. Preparation and characterization of monodisperse zirconia spherical nanometer powder via lamellar liquid crystal template method[J]. , 2015, 23(10): 1721-1727.
Weiyan He, Jinrong Liu, Zhenzhu Cao, 等. Preparation and characterization of monodisperse zirconia spherical nanometer powder via lamellar liquid crystal template method[J]. 中国化学工程学报（英文版）, 2015,23(10):1721-1727. DOI： 10.1016/j.cjche.2015.08.032.

Weiyan He, Jinrong Liu, Zhenzhu Cao, Caihong Li, Yanfang Gao. Preparation and characterization of monodisperse zirconia spherical nanometer powder via lamellar liquid crystal template method[J]. , 2015, 23(10): 1721-1727. DOI： 10.1016/j.cjche.2015.08.032.

摘要

Abstract

Cubic phase spherical zirconia nano-powderwas prepared by a direct template route in the lamellar liquid crystal formed by polyoxyethylene

tert

-octylphenyl ether (Triton X-100)/sodium dodecyl sulfate (SDS)/H

O. The precursor powder and zirconia powder were characterized by XRD

FT-IR

TG/DSC

TEM

and SEM methods. Results show that the stability of the lamellar liquid crystal is controlled by NH

· H

O concentration. The size of nanoparticles is greatly affected by NH

·H

Oand ZrOCl

· 8H

O concentrations. The zirconia nanoparticles shownarrow particle size distribution of 10-30 nm.

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