Jianhui Zhou, Xiaotong Zhang, Ying Yan, Jianfeng Hu, Hang Wang, Yan Cai, Jinqing Qu. Preparation and characterization of a novel antibacterial acrylate polymer composite modified with capsaicin[J]. Chinese Journal of Chemical Engineering, 2019, 27(12): 3043-3052.
DOI:
Jianhui Zhou, Xiaotong Zhang, Ying Yan, Jianfeng Hu, Hang Wang, Yan Cai, Jinqing Qu. Preparation and characterization of a novel antibacterial acrylate polymer composite modified with capsaicin[J]. Chinese Journal of Chemical Engineering, 2019, 27(12): 3043-3052.DOI: 10.1016/j.cjche.2019.03.024.
Preparation and characterization of a novel antibacterial acrylate polymer composite modified with capsaicin
A novel antibacterial acrylate polymer composite modified with capsaicin was successfully synthesized by a two-step reaction. Capsaicin and acryloyl chloride were firstly esterified
and then applied to solution polymerization with acrylate monomers and styrene. The yield of the esterified products was about 85.3%. The polymer was characterized by Fourier transform infrared spectroscopy (FTIR)
gel permeation chromatography (GPC)
thermogravimetric analysis (TGA)
contact angle (CA) and antibacterial ring tests. The number-average molecular weight (
M
n
) of the polymer was 27214
based on the capsaicin-acrylate dosage of 6.5 wt%. The TGA revealed a stable thermal property. The contact angles of the polymers films on tinplate increased from 77.5° to 86.2° with the increasing amount of capsaicin-acrylate. The antibacterial tests demonstrated excellent antimicrobial capability of the polymers.
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