CAI Shuangfei, WANG Lisheng, YAN Guoqing, LI Yi. Solubilities of 1-Methyl-3-(3-sulfopropyl)-imidazolium Hydrogen Sulfate in Selected Solvents[J]. , 2010, 18(6): 1008-1012.
DOI:
CAI Shuangfei, WANG Lisheng, YAN Guoqing, LI Yi. Solubilities of 1-Methyl-3-(3-sulfopropyl)-imidazolium Hydrogen Sulfate in Selected Solvents[J]. , 2010, 18(6): 1008-1012.DOI: 10.1016/S1004-9541(09)60160-9.
Solubilities of 1-Methyl-3-(3-sulfopropyl)-imidazolium Hydrogen Sulfate in Selected Solvents
) was synthesized and characterized by infrared spectroscopy(IR)
nuclear magnetic resonance(
1
H and
13
C NMR) and ultraviolet-visible(UV-Vis) spectra. Its thermal stability was also examined by thermogravimetric analysis(TGA) and a differential scanning calorimeter(DSC). The mole fraction solubilities of [C
3
SO
3
HMIM
]
[HSO
4
]
) in 12 selected solvents(
n
-pentane
n
-hexane
n
-heptane
benzene
toluene
ethylbenzene
acetone
2-butanone
3-methyl-2-butanone
tetrahydrofuran
ethyl acetate and dichloromethane) in the temperature range from 289.15 to 363.15 K were measured using a static analytical method and correlated with an empirical equation.
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